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LaMotte DC1600 Colorimeter User Manual

Page 84

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PROCEDURE

1.

Rinse a clean colorimeter tube (0967) with sample water. Fill to the 10 mL line with sample.

2.

Select setting 5 on “Select Wavelength” knob and press “30 Second Read” button.

3.

Insert tube into colorimeter chamber and adjust to 100%T with “Set Blank” knob. This is the 100%T blank.

4.

Remove tube from colorimeter. Use the 1.0 mL pipet (0354) to add 1.0 mL of *Sulfide Reagent A (V-4458). Cap and

mix.

5.

Add 6 drops of *Sulfide Reagent B (V-4459). Cap and mix. Wait 1 minute. Solution will turn blue if sulfides are

present.

6.

Use the 1.0 mL pipet (0354) to add 2.0 mL of Sulfide Reagent C (4460). Cap and mix. Color development is

immediate and stable.

7.

Press “30 Second Read” button and insert tube into colorimeter chamber. Record %T as soon as reading stabilizes.

8.

Consult calibration chart to determine sulfide concentration in parts per million (ppm) .

DC1600 SULFIDE CALIBRATION CHART

%T

9

8

7

6

5

4

3

2

1

0

90

0.00

0.02

0.03

0.05

0.06

0.08

0.09

80

0.11

0.12

0.14

0.15

0.17

0.19

0.20

0.22

0.23

0.25

70

0.27

0.29

0.30

0.32

0.34

0.36

0.37

0.39

0.41

0.43

60

0.45

0.47

0.49

0.51

0.53

0.55

0.57

0.59

0.61

0.63

50

0.65

0.67

0.70

0.72

0.74

0.76

0.79

0.81

0.84

0.86

40

0.89

0.91

0.94

0.96

0.99

1.02

1.04

1.07

1.10

1.13

30

1.16

1.19

1.22

1.25

1.29

1.32

1.35

1.39

1.43

1.46

20

1.50

1.54

1.58

1.62

1.66

1.70

1.75

1.80

1.84

1.89

10

1.95

2.00

2.06

2.12

2.18

2.24

2.31

2.38

2.46

2.54

0

2.63

2.73

2.83

2.95

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