3 replacing parts of the msm – Metrohm 850 Professional IC Anion MCS LP-Gradient User Manual
Page 110
5.11 Metrohm Suppressor Module (MSM)
■■■■■■■■■■■■■■■■■■■■■■
100
■■■■■■■■
850 Professional IC – Anion – MCS – LP Gradient
5.11.3.3
Replacing parts of the MSM
It may be necessary to replace parts of the MSM in the following cases:
■
Loss of suppression capacity which cannot be eliminated (reduced
phosphate sensitivity and/or significant rise in the baseline).
■
Blockage of the MSM which cannot be eliminated (solutions can no
longer be pumped through the suppressor).
Both the MSM rotor A (50-3) and the MSM connecting piece (50-2) with
its supply and discharge lines can be replaced.
Replacing parts of the MSM
Replace parts of the MSM as follows (see Figure 50, page 98):
1 Disconnecting the MSM from the IC system
■
Switch off the instrument.
■
Disconnect the MSM from the separation column, peristaltic
pump and detector.
2 Dismantling the MSM
■
Unscrew union nut (50-1) from the MSM housing (50-4).
■
Pull MSM connecting piece (50-2) and MSM rotor A (50-3) out of
the MSM housing (50-4). The MSM connecting piece and MSM
rotor A normally stick to one another - if this is not the case: Take
a sharp object, insert into the slot (50-5) in the MSM housing,
and pull out MSM rotor A (50-3) in this way.
■
Detach the MSM connecting piece (50-2) from MSM rotor A
(50-3).
3 Cleaning the new MSM rotor A
■
Clean the sealing surface of the new MSM rotor A (50-3) with
ethanol using a lint-free cloth.
4 Inserting the new MSM rotor A
Caution
An incorrectly inserted MSM rotor A (50-3) can be destroyed
during start-up.