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4-1. preparation – Yokogawa DO202 2-Wire Dissolved Oxygen Analyzer User Manual

Page 55

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IM 12J05C01-01E

6-4 Calibration Procedure

6-4. Calibration procedure using manual calibra-

tion method

6-4-1. Preparation

A. Cleaning

Confirm that the readings of the analyzer are

stable and measured with a clean sensor.

Otherwise move the sensor to a maintenance site

and wash off any dirt on the sensor membrane

Move the sensor back to the process water and

wait for the readings to stabilize.

B. Sampling

The manual calibration procedure involves

adjustment of the readings to a reference standard.

Normally this reference is a laboratory

measurement that analyses a sample that must

be identical to the sample measured with the on-

line analyzer.

The following precautions must be taken into

account:

• The sample must be analyzed directly after

sampling to avoid change of dissolved oxygen

concentration or temperature after sampling

• The reference standard must be analyzed with

a laboratory meter that is calibrated prior to

sample analysis

• The reference method must be calibrated with

the same calibration data as specified in ISO

5814 to avoid indiscrepancies

Most important calibration data are:

Dissolved oxygen concentration at saturation

conditions as function of temperature, barometric

pressure, altitude and salinity.

These data are included in this manual for

reference and verification of correct calibration of

reference analyzers. DO202 has taken all these

variables into account during the semi-automatic

calibration methods.

6-4-2. Procedure for manual slope (sensitivity) calibration

NO

YES

ENT

NO

YES

NO

YES

Select the flashing digit with the key.

Increase its value by pressing the key.

When the correct value is displayed,

press ENT to enter the change.

After briefly displaying WAIT,

the display returns to

the normal readout.

YES

Press YES to return to the

measuring mode. (Single Point

adjustment only)

ENT

ENT

ENT

YES

YES

ENT

FAIL

TEMP.MAN

YES NO

ENT

NO

MODE

YES

MODE

%sat

ppb

CAL
DISPLAY

ppm

HOLD

OUTPUT

SET HOLD

SERVICE