Parr Instrument Series 4558 - Manual (Page 3)

4555 - 58 Series
5G & 10L Pressure Reactors
- 2 -
TABLE OF CONTENTS
TABLE OF CONTENTS ............................ 2
Related
Instructions........................... 3
Customer Service .............................. 3
PREFACE ................................................. 4
Scope ................................................ 4
Safety
Information ............................. 4
Provisions for Lifting and Carrying..... 4
General Specifications....................... 5
Explanation of Symbols ..................... 6
Environmental Conditions.................. 6
Intended Usage ................................. 7
User’s Responsibility ......................... 7
Unpack Carefully ............................... 7
INSTALLATION ........................................ 8
Pressure,
Temperature Limits ........... 8
Slave Box Control A1761HC3 ........... 8
ASSEMBLE THE REACTOR.................... 9
Removable
Head Vessel ................... 9
Fixed Head Vessel .......................... 10
Cylinder Slide Adjustment................ 12
IDENTIFY THE VALVES......................... 13
Gas
Inlet Valve ................................ 13
Gas Release Valve .......................... 13
Liquid Sampling Valve ..................... 13
OTHER VESSEL HEAD FITTINGS ........ 14
Safety
Rupture Disc......................... 14
Type J Thermocouple ...................... 14
Pressure Gage ................................ 14
Gage and Valve Adapters................ 14
HOW TO USE THE VESSEL .................. 15
Flat Gasket or O-ring Seal ............... 15
To Open the Vessel ......................... 15
Before Closing the Vessel ............... 15
Close the Vessel.............................. 16
Gas Connections ............................. 16
Pressurizing the Vessel ................... 16
Do Not Overfill ................................. 17
Releasing Pressure ......................... 17
Withdrawing Liquid Samples............ 17
The Shaft Seal ................................. 17
REACTORS WITH SLAVE BOX CONTROLS 18
3-Zone Slave Box A1761HCEE ........ 18
3-Zone Slave Box A1761HC3 ........... 18
Initial Operating Test......................... 18
ACCESSORIES........................................ 19
Internal
Cooling Coils........................ 19
Stirrer Drive Systems ........................ 19
Quick Disconnect Drive Coupler ....... 19
Air Motor ........................................... 20
Variable Speed Electric Motor .......... 20
Spare Parts Kit.................................. 20
EXPLOSION PROOF OPERATION ......... 21
The
Motor ......................................... 21
The Temperature Controller.............. 21
Slave Box Control ............................. 21
The Heater ........................................ 21
The Wiring ........................................ 21
PERIODIC PRESSURE TESTS ............... 22
GENERAL MAINTENANCE NOTES........ 23
Fuses ................................................ 24
PARTS LISTS........................................... 25
Vessel
Parts List ............................... 25
Internal Fittings ................................. 25
External Fittings ................................ 26
Internal Parts Identification ............... 27
External Parts Identification .............. 28
Cooling Coils & Fittings..................... 29
Drive Parts List.................................. 30
Stands............................................... 31
Slave
Boxes ...................................... 31
Heaters ............................................. 32
APPENDIX A – REMOVABLE VESSEL
REACTOR DRAWINGS ........................... 33
APPENDIX B – FIXED HEAD VESSEL
REACTOR DRAWINGS ........................... 36