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850 professional ic – Metrohm VoltIC pro I User Manual

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Application Bulletin 356

Installation instruction for «VoltIC pro I»

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Fig.: Electrical connection diagram for the VoltIC pro I system

2.2 850 Professional IC

In order to install the Professional IC you have to perform

the following steps: Remove rollers and handle, place the

detector blocks in the instrument and connect the detector

cables, remove transport locking screws, connect the leak

sensor cable, connect the drainage tubing, and set up the

eluent bottles. Please refer to the 850 Professional IC

manual for a detailed description (chapters 2.6 and 2.8).

Capillaries are connected according to the following list and

the diagram below (also see manual chapters 2.14 to 2.18)

1. Connection to the eluent bottle for anion determination

2. Capillary to anion separation column

3. MSM inlet capillary

– labeled with Eluent

4. MSM outlet capillary

– labeled with Detector, which can

be connected to the MCS or directly to the detector.

The MCS air aspiration capillary is connected to the

CO

2

-absorber cartridge.

5. Capillary from MCS to anion detector, long PEEK

pressure screws (6.2744.090) are used for the MCS

connection

6. Detector outlet capillary to waste

7. Regeneration solution aspiration capillaries (PTFE, 0.97

mm ID), connected to two bottles with ultrapure water

and 50 mmol/L sulfuric acid respectively via peristaltic

pump tubing with orange/yellow stoppers (6.1826.320)

8. MSM regeneration solution outlet capillaries

– labeled

with Waste

– to waste

9. Connection to the Eluent bottle for cation determination

10. Capillary to cation separation column

11. Capillary from cation separation column to cation

detector

12. Detector outlet capillary to waste

13. Sample inlet capillary (PTFE, 90 cm, d=0.25 mm),

connected to the anion valve (position 1)

14. Optional sample degasser

Capillary connection (PTFE, 40 cm, d=0.5 mm) between

anion valve (position 2) and cation valve (position 1)

15. Connection capillary anion channel valve to cation

channel valve

16. Capillary to the waste