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Metrohm 882 Compact IC plus – Cation User Manual

Page 6

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Table of contents

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IV

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882 Compact IC plus – Cation

3.12 Injection valve ..................................................................... 31
3.12.1

Connecting the injection valve ............................................... 31

3.12.2

Mode of operation of the injection valve ............................... 33

3.12.3

Selecting the sample loop ...................................................... 34

3.13 Connecting the instrument ................................................ 34
3.13.1

Connecting the instrument to the PC ..................................... 34

3.13.2

Connecting the instrument to mains supply ........................... 34

3.14 Guard column ..................................................................... 35

3.15 Separation column ............................................................. 37

4 Start-up

39

4.1

Initial start-up ..................................................................... 39

4.2

Conditioning ........................................................................ 40

5 Handling and maintenance

42

5.1

General notes ...................................................................... 42

5.1.1

Care ...................................................................................... 42

5.1.2

Maintenance by Metrohm Service .......................................... 42

5.1.3

Operation .............................................................................. 43

5.1.4

Shutting down ...................................................................... 43

5.2

Capillary connections ......................................................... 43

5.2.1

Operation .............................................................................. 43

5.3

Door ..................................................................................... 44

5.4

Eluent ................................................................................... 44

5.4.1

Production ............................................................................. 44

5.4.2

Operation .............................................................................. 45

5.5

High pressure pump ........................................................... 45

5.5.1

Protection ............................................................................. 45

5.5.2

Maintenance ......................................................................... 46

5.6

Inline filter ........................................................................... 56

5.6.1

Maintenance ......................................................................... 56

5.7

Injection valve .................................................................... 58

5.7.1

Protection ............................................................................. 58

5.8

Inline sample preparation .................................................. 58

5.9

Rinsing the sample path .................................................... 58

5.10 Separation column ............................................................. 60
5.10.1

Separating efficiency .............................................................. 60

5.10.2

Protection ............................................................................. 60

5.10.3

Storage ................................................................................. 60

5.10.4

Regeneration ......................................................................... 61

5.11 Quality Management and validation with Metrohm ....... 61