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Metrohm 930 Compact IC Flex Oven/ChS/PP/Deg User Manual

Page 6

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Table of contents

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IV

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930 Compact IC Flex Oven/ChS/PP/Deg (2.930.2360)

3.13 Peristaltic pump .................................................................. 36
3.13.1

Installing the peristaltic pump ................................................ 36

3.13.2

Mode of operation for the peristaltic pump ........................... 41

3.14 Installing the detector ........................................................ 42

3.15 Connecting the sample degasser (optional) ..................... 43

3.16 Connecting the instrument to a computer ....................... 45

3.17 Connecting the instrument to the power supply ............. 46

3.18 Initial start-up ..................................................................... 47

3.19 Connecting and rinsing the guard column ....................... 49

3.20 Connecting the separation column ................................... 51

3.21 Conditioning ........................................................................ 55

4 Operation

57

5 Operation and maintenance

58

5.1

IC system ............................................................................. 58

5.1.1

Operation .............................................................................. 58

5.1.2

Care ...................................................................................... 58

5.1.3

Maintenance by Metrohm Service .......................................... 58

5.1.4

Shutting down and starting back up ...................................... 59

5.2

Capillary connections ......................................................... 60

5.3

Servicing the door .............................................................. 60

5.4

Column oven – replacing the capillaries ........................... 60

5.5

Handling the eluent ............................................................ 62

5.5.1

Manufacturing eluent ............................................................ 62

5.5.2

Changing the eluent .............................................................. 63

5.6

Servicing the eluent degasser ........................................... 63

5.7

Notes on operating the high-pressure pump ................... 64

5.8

Servicing the high-pressure pump .................................... 65

5.9

Servicing the inline filter .................................................... 78

5.10 Servicing the pulsation absorber ...................................... 81

5.11 Injection valve ..................................................................... 81

5.12 Suppressor .......................................................................... 81
5.12.1

Notes for operating the suppressor ........................................ 81

5.12.2

Taking care of the suppressor housing ................................... 82

5.12.3

Servicing the suppressor ........................................................ 82

5.13 Peristaltic pump .................................................................. 89
5.13.1

Notes on operating the peristaltic pump ................................ 89

5.13.2

Servicing the peristaltic pump ................................................ 89

5.14 Servicing the detector ........................................................ 91