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Media preparation, Cartridge preparation, For laboratory use – SKC DCS (Deployable Cartridge Sampler) System User Manual

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MEDIA PREPARATION

For Laboratory Use

Use clean hexane-rinsed PTFE-tipped forceps to handle fi lters.

Wear disposable, clean, lint-free nylon or powder-free surgical gloves
to handle the sorbent and cartridge.

Quartz Filter: Prepare following the procedure outlined in EPA TO-9A or
TO-13A, Section 10.2.1. (htt p://www.epa.gov/tt namti1/airtox.html)

XAD-2 Sorbent: Purchase precleaned or use procedure outlined in EPA TO-
13A, Section 10.2.5.

PUF: Purchase precleaned or use procedure outlined in EPA TO-9A or TO-13A,
Section 10.2.4.

CARTRIDGE PREPARATION

For Laboratory Use

Use clean hexane-rinsed PTFE-tipped forceps to handle fi lters.

Wear disposable, clean, lint-free nylon or powder-free surgical gloves
to handle the sorbent and cartridge.

1. Rinse cartridge with appropriate organic solvent and allow to dry.
2. Ensure PTFE gasket 1, the stainless steel support screen 1, and PTFE

gasket 2 are in place on bott om cartridge cap.

3. Insert PUF or XAD-2 into the cartridge.
4. Ensure the PTFE gasket 3 and stainless

steel screen 2 are in place on cartridge
body top.

5. Using cleaned forceps, align quartz fi lter

with screen radially, and place PTFE
gasket 4 on top of fi lter. Thread top
cartridge cap onto cartridge.

6. Wrap the cartridge with hexane-rinsed

aluminum foil, place in supplied PTFE
jar, and label jar. Analyze (certify) at least
1 cartridge from each batch of cartridges
prepared using the procedure described
in Section 10.3 of EPA TO-9A or EPA
TO-13A (htt p://www.epa.gov/tt namti1/
airtox.html) prior to fi eld use. See Section
10.3.8 for acceptable background levels.
Cartridges are considered clean for up to
30 days from date of certifi cation when
sealed in their containers.

Cartridge for EPA TO-13A

Top

cartridge cap

PTFE gasket 4

Stainless steel

support screen 2

PTFE gasket 3

Stainless steel
cartridge body

PTFE gasket 2

Stainless steel

support screen 1

Bottom

cartridge cap

Insert

47-mm

fi lter

Insert

PUF or

XAD-2

sorbent

t

t

PTFE gasket 1