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Metrohm 930 Compact IC Flex Oven/SeS/PP User Manual

Page 6

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Table of contents

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IV

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930 Compact IC Flex Oven/SeS/PP (2.930.2500)

3.12.2

Mode of operation for the peristaltic pump ........................... 40

3.13 Metrohm CO

2

Suppressor (MCS) ....................................... 41

3.13.1

General information on MCS ................................................. 41

3.13.2

Connecting the MCS ............................................................. 42

3.13.3

Installing adsorption cartridges .............................................. 43

3.14 Installing the detector ........................................................ 45

3.15 Connecting the instrument to a computer ....................... 45

3.16 Connecting the instrument to the power supply ............. 46

3.17 Initial start-up ..................................................................... 47

3.18 Connecting and rinsing the guard column ....................... 50

3.19 Connecting the separation column ................................... 52

3.20 Conditioning ........................................................................ 55

4 Operation

57

5 Operation and maintenance

58

5.1

IC system ............................................................................. 58

5.1.1

Operation .............................................................................. 58

5.1.2

Care ...................................................................................... 58

5.1.3

Maintenance by Metrohm Service .......................................... 58

5.1.4

Shutting down and starting back up ...................................... 59

5.2

Capillary connections ......................................................... 60

5.3

Servicing the door .............................................................. 60

5.4

Column oven – replacing the capillaries ........................... 60

5.5

Handling the eluent ............................................................ 62

5.5.1

Manufacturing eluent ............................................................ 62

5.5.2

Changing the eluent .............................................................. 63

5.6

Notes on operating the high-pressure pump ................... 63

5.7

Servicing the high-pressure pump .................................... 64

5.8

Servicing the inline filter .................................................... 77

5.9

Servicing the pulsation absorber ...................................... 80

5.10 Injection valve ..................................................................... 80

5.11 Suppressor .......................................................................... 80
5.11.1

Notes for operating the suppressor ........................................ 80

5.11.2

Taking care of the suppressor housing ................................... 81

5.11.3

Servicing the suppressor ........................................................ 81

5.12 Peristaltic pump .................................................................. 88
5.12.1

Notes on operating the peristaltic pump ................................ 88

5.12.2

Servicing the peristaltic pump ................................................ 88

5.13 Servicing the Metrohm CO

2

Suppressor (MCS) ................ 90

5.13.1

Replacing the CO

2

adsorption cartridge ................................. 90