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Metrohm 850 Professional IC Cation - Gradient User Manual

Page 6

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Table of contents

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IV

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850 Professional IC Cation – HP-Gradient

3.11 Inline filter ........................................................................... 37

3.12 Pulsation damper ............................................................... 38

3.13 Sample degasser ................................................................. 39

3.14 Injection valve ..................................................................... 41
3.14.1

Connecting the injection valve ............................................... 41

3.14.2

Mode of operation of the injection valve ............................... 42

3.14.3

Selecting the sample loop ...................................................... 43

3.15 Column thermostat ............................................................ 43

3.16 Connecting the instrument ................................................ 46
3.16.1

Connecting the instrument to the PC ..................................... 46

3.16.2

Connecting the instrument to mains supply ........................... 46

3.17 Guard column ..................................................................... 47

3.18 Separation column ............................................................. 48

4 Start-up

50

4.1

Initial start-up ..................................................................... 50

4.2

Conditioning ........................................................................ 51

5 Operation and maintenance

53

5.1

General information ........................................................... 53

5.1.1

Care ...................................................................................... 53

5.1.2

Maintenance by Metrohm Service .......................................... 53

5.1.3

Operation .............................................................................. 54

5.1.4

Shutting down ...................................................................... 54

5.2

Capillary connections ......................................................... 54

5.2.1

Operation .............................................................................. 54

5.3

Door ..................................................................................... 54

5.4

Eluent ................................................................................... 55

5.4.1

Production ............................................................................. 55

5.4.2

Operation .............................................................................. 55

5.5

High pressure pump ........................................................... 56

5.5.1

Protection .............................................................................. 56

5.5.2

Maintenance ......................................................................... 56

5.6

Inline filter ........................................................................... 67

5.6.1

Maintenance ......................................................................... 67

5.7

Inline sample preparation .................................................. 69

5.8

Rinsing the sample path .................................................... 69

5.9

Sample degasser ................................................................. 71

5.9.1

Operation .............................................................................. 71

5.10 Injection valve .................................................................... 71
5.10.1

Protection .............................................................................. 71