Carbolite TZF Series - Manual (Page 8)

1700-1800° Tube
8
MF32 - 3.25
C. Independent Control
In this case the three controllers are completely independent. Note that it is not possible to
maintain very different zone temperatures because of heat transfer within the work tube.
3.4 General Operating Advice
Heating element life is shortened by use at temperatures close to maximum. Do not leave the
furnace at high temperature when not required. The maximum temperature is shown on the furnace
rating label and on the back page of this manual. The furnace can be cycled between room
temperature and maximum without a detrimental effect on element life - but see the notes on tube
life.
On first installing the elements, and on subsequent element replacement, run the furnace at 1500°C
for an hour to create a protective glaze on the element surface.
The furnace elements are very susceptible to mechanical shock. Take great care when moving the
furnace.
Lightweight ceramic fibre insulation can easily be marked by accidental contact. Some fine cracks
may be visible on the surface of the insulation, or may develop in the surface of the chamber due
to the progressive shrinkage of the insulation materials. Cracks are not usually detrimental to the
functioning or the safety of the furnace.
3.5 Operator Safety
Ceramic materials used in furnace manufacture can become conduction at high temperature. Avoid
using conductive tools within the work tube without first isolating the elements. The elements are
isolated (via a contactor) when the instrument switch is off.
If a metal work tube is used, it must be earthed (grounded). Note that the furnace temperature
should be limited if a metal tube is used.
Ensure that there are no inflammable objects placed in such a way that the work tube could break
and fall on them.
3.6 Tube Life
A ceramic work tube may crack if workpieces are inserted
too quickly or at temperatures below 900°C (when the tube
is more brittle). Large pieces should also be heated slowly
to ensure that large temperature differences do not arise.
Poor thermal contact should be encouraged between the
workpiece and the tube; crucibles or boats should be of
low thermal mass and should have feet to reduce the
contact with the tube (fig. 4).
Avoid metal directly touching the work tube - see the safety warning above.
Do not set too high a heating rate. Large diameter tubes are more susceptible to thermal shock than
smaller. A general rule for maximum heating rate is 400/internal diameter (°C/min); for 75mm i/d
tubes this comes to 5°C per minute. The controller can be set to limit the heating rate.
3.7 Pressure
Work tubes are not able to accept high internal pressure. When gas seals or similar fittings are in
use, the gas pressure should be restricted to a maximum of 0.2 bar (3 psi). A pressure of about half
of that should normally be sufficient to achieve the desired flow rate. The customer must ensure
that the exhaust path from the tube is not blocked, so that excess pressure does not occur.
3.8 Thermocouples - Warnings
(1) The output from 1700-1800°C thermocouples when used regularly at temperatures greater than
1650°C can deteriorate and decrease with age.