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Teledyne 6000A - Photometric analyzer User Manual

Page 40

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3 Operation

Model 6000A

3-16 Part I

Teledyne Analytical Instruments

Readjust the gas pressure into the analyzer until the flowrate through the

Sample Cell settles between 50 to 200 cc/min (approximately 0.1 to 0.4
SCFH).

Note: Always keep the calibration gas flow as close to the flowrate of

the sample gas as possible

3.4.1 Zero Cal

The

Zero

button on the front panel is used to enter the zero calibration

function. Zero calibration can be performed in either the automatic or manual
mode.

Make sure the zero gas is flowing to the instrument. If you get a

CELL

CANNOT BE BALANCED message while zeroing skip to section 4.4.1.3.

3.4.1.1

Auto Mode Zeroing

Observe the precautions in sections 4.4 and 4.4.1, above. Press

Zero

to

enter the zero function mode. The screen allows you to select whether the zero
calibration is to be performed automatically or manually. Use the

∆∇ arrow

keys to toggle between

AUTO and MAN zero settling. Stop when AUTO appears,

blinking, on the display.

Select zero

mode: AUTO

Press

Enter

to begin zeroing.

####.## %

SO2

Slope=#.### C—Zero

The beginning zero level is shown in the upper left corner of the display. As

the zero reading settles, the screen displays and updates information on

Slope=

in percent/second (unless the Slope starts within the acceptable zero range and
does not need to settle further). The system first does a coarse zero, shown in
the lower right corner of the screen as

C—Zero, for 3 min, and then does a fine

zero, and displays

F—Zero, for 3 min.

Then, and whenever Slope is less than 0.01 for at least 3 min, instead of

Slope you will see a countdown:

9 Left, 8 Left, and so fourth. These are software

steps in the zeroing process that the system must complete, AFTER settling,
before it can go back to

Analyze

. Software zero is indicated by

S–Zero in the

lower right corner.