IKA C 2000 control User Manual
Page 46
3UHSDULQJ DQG SHUIRUPLQJ PHDVXUHPHQWV
IKA
-WERKE C 2000 basic / control
Ver. 04 08.07
3DJH
(DFK GHFRPSRVLWLRQ YHVVHO PXVW EH FRGHG EHIRUH WKH ILUVW WLPH LW LV XVHG
To do this, attach the black code rings into the recesses of the decomposition vessel
provided for that purpose.
1RWHV RQ WKH VDPSOH
'HFRPSRVLWLRQ YHVVHOV & DQG & DUH QRW SHUPLWWHG IRU H[SHULPHQWV RQ
IXHO VDPSOHV FDSDEOH RI H[SORGLQJ 1RWH LQ WKLV UHJDUG &KDSWHU ³)RU \RXU VDIHW\´
7KH LQGLYLGXDO SDUWV DQG LQ SDUWLFXODU WKH WKUHDGLQJ RI WKH GHFRPSRVLWLRQ YHVVHO
PXVW EH FKHFNHG UHJXODUO\ IRU ZHDU DQG FRUURVLRQ 1RWH LQ WKLV UHJDUG 2SHUDWLQJ
,QVWUXFWLRQV & RU &
The C 2000 calorimeter system is a precision measuring instrument for routine de-
termination of gross calorific values of solid and liquid substances. Exact measure-
ments are only possible, however, if the individual steps of the experiment are fol-
lowed carefully. The procedure as it is described in Chapter 1 “For your safety” and
in the following sections must therefore be followed precisely.
,I PRUH WKDQ RQH GHFRPSRVLWLRQ YHVVHO LV EHLQJ XVHG WKH UHVSHFWLYH LQGLYLG
XDO SDUWV PXVW QRW EH H[FKDQJHG EHWZHHQ WKH YDULRXV GHFRPSRVLWLRQ YHVVHOV
VHH WKH HQJUDYLQJ RQ WKH LQGLYLGXDO SDUWV
Substances of which the combustion behavior is not known must be examined for
their combustion behavior before combustion in the decomposition vessel C 5010,
C 5012 or C 62 (danger of explosion). If you are burning
XQNQRZQ VDPSOHV
, leave
the room or
NHHS D VDIH GLVWDQFH
between you and the calorimeter.
A few points must be observed in reference to the substances to undergo combus-
tion. Normally, solid substances can be burned directly in powder form. Substances
that burn rapidly (for example benzoic acid) must not be burned in loose form.
Benzoic acid must only be burned in the form of pellets! Combustible dust and pow-
der must be compressed into pellets before combustion. Oven-dry dust and powder
such as wood chips, hay, straw, etc. burn in an explosive manner! They must be
moistened first! Readily combustible liquids with a low vapor pressure must not be
come in direct contact with the cotton thread (for example tetramethyl dihydrogen
disiloxan)!
☞
Decomposition vessel No:
(without coding)
recess for
code ring
☞
FRGLQJ RI WKH
GHFRPSRVLWLRQ
YHVVHOV
VROLG
VXEVWDQFHV
☞
QRWHV RQ WKH
VDPSOH