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Identify the valves, Gas inlet valve, Gas release valve – Parr Instrument 4575/76 HP/HT User Manual

Page 8: Liquid sampling valve

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P a r r I n s t r u m e n t C o m p a n y

4575/76 HP/HT Pressure Reactors

8

Pressure Gage

Magnetic Drive

Thermocouple

/ Thermowell

Head

Thermocouple /

Thermowell

Cooling Loop

Propellers

Stirring Shaft

Dip Tube

Liquid

Sampling

Valve

Gas Inlet Valve

Gas Release Valve

Fixed Head

Identify the Valves

Gas Inlet Valve

The gas inlet valve is easily identified when the
bomb is open by noting that it is connected to a dip
tube which extends to a point near the bottom of
the cylinder. This valve has an attached fitting which
provides a socket for attaching the A506HC pressure
hose furnished with the reactor.

Gas Release Valve

The gas release valve is installed on the gage adapt-
er. Gas released from this valve will be drawn from
the head space of the vessel.

Liquid Sampling Valve

The liquid sampling valve is attached to the same
fitting as the gas inlet valve and connected to the
same dip tube. With this arrangement, incoming gas
is always introduced below the surface of the liquid
and the operator is provided with a means for clear-
ing the dip tube to be sure that any sample taken
during a run will be representative of the charge.
This can be done by opening the upper gas inlet
valve momentarily to allow the inlet gas to force any
liquid in the dip tube back into the reactor before
withdrawing a sample from the sampling valve.