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Chapter 3: getting started – Labconco CentriVap Centrifugal Concentrators and Cold Traps 74750 Series User Manual

Page 17

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Chapter 3: Getting Started

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13

Acids Bases Solvents

COMPONENT MATERIAL

Acetic Acid 20%

Boric Acid

F

or

m

ic Acid

H

ydrobromic Acid 20%

H

ydrochloric Acid 20%

Nitr

ic Acid 20%

Sulfur

ic Acid 10

%

Trifluoroacetic Acid

(TFA

)

Ammonium H

ydr

oxide

Acetone

Acetonitrile

Chl

oroform

Dimeth

yl F

or

m

amide

Dimeth

yl Sulfoxide

Ethanol

Eth

yl Acetate

Hexanes

Iso

pro

ponal

Methanol

Meth

ylene Chloride

Meth

yl t-

But

yl Ether

Toluene

Wate

r

Rotor Hub

Acetal

C C C D D D C

D C

Chamber &
Cold Trap Lid

Acrylic

C D C D D D D C D D C D D

Chamber

Epoxy coated
Aluminum

C

D

C D

Tubing

PVC

D C D D D D D D C D D D D

Lid Gasket

EPDM

D

D

C

D

Cold Trap
Gasket

Neoprene

D

D C D D C D D D D D C D

Rotor

Anodized
Aluminum

D D

Rotor Shaft &
Cold Trap

Stainless
Steel

D D

D

Bearings

High Carbon
Steel

D D D D D D D

D

D

C-Moderate Degradation - Questionable use
D-Severe Degradation - Infrequent use recommended - immediate thorough

neutralizing and cleaning is required.

• If a rotary vane vacuum pump is used, frequent oil changes are required.

Most compounds used in the CentriVap will degrade the oil if allowed to
enter to pump.

• Diaphragm vacuum pumps sold by Labconco have wetted parts either made

from PTFE or protected by PTFE coatings and are suitable for nearly all
procedures.

• When using compounds in the CentriVap that are hostile to the materials of

construction, it is imperative that the equipment is appropriately maintained.
After each run, clean up all residues, spills and materials that might have
splashed in the chamber.

• Drain the Cold Trap immediately after the collected ice is melted to prevent

corrosive liquids from residing in the trap. Flush out the trap with water after
draining.

DO NOT chip ice off the Cold Trap walls as damage may occur.

DO NOT start a rotary vane pump when the Cold Trap contains any liquid.
The liquid will be drawn into the pump and will contaminate the vacuum
pump oil.