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Metrohm 850 Professional IC Anion MCS Prep 1 User Manual

Page 7

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Table of contents

850 Professional IC – Anion – MCS – Prep 1

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V

4.6

Inline filter ........................................................................... 85

4.6.1

Maintenance ......................................................................... 85

4.7

Inline sample preparation .................................................. 87

4.8

Rinsing the sample path .................................................... 87

4.9

Sample degasser ................................................................. 89

4.9.1

Operation .............................................................................. 89

4.10 Injection valve .................................................................... 89
4.10.1

Protection .............................................................................. 89

4.11 Metrohm Suppressor Module (MSM) ............................... 89
4.11.1

Protection .............................................................................. 89

4.11.2

Operation .............................................................................. 89

4.11.3

Maintenance ......................................................................... 90

4.12 Peristaltic pump .................................................................. 95
4.12.1

Operation .............................................................................. 95

4.12.2

Maintenance ......................................................................... 96

4.13 Metrohm CO

2

suppressor (MCS) ....................................... 98

4.13.1

Replacing the CO

2

adsorption cartridge ................................. 98

4.13.2

Regenerating the H

2

O adsorption cartridge ............................ 98

4.14 Conductivity detector ......................................................... 99
4.14.1

Maintenance ......................................................................... 99

4.15 Separation column ............................................................. 99
4.15.1

Separating efficiency .............................................................. 99

4.15.2

Protection ............................................................................ 100

4.15.3

Storage ............................................................................... 100

4.15.4

Regeneration ....................................................................... 100

4.16 Quality Management and validation with Metrohm .... 101

5 Troubleshooting

102

5.1

Problems and their solutions .......................................... 102

6 Technical specifications

107

6.1

Reference conditions ........................................................ 107

6.2

Instrument ......................................................................... 107

6.3

Leak sensor ....................................................................... 107

6.4

Ambient conditions .......................................................... 107

6.5

Housing ............................................................................. 108

6.6

Eluent degasser ................................................................ 108

6.7

High pressure pump ......................................................... 108

6.8

Sample degasser ............................................................... 109

6.9

Injection valve ................................................................... 109