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Metrohm TitrIC pro I User Manual

Page 8

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Fig


Co
to

tran
He

6.2

Go

Tow
pos

(cli

6.2

A s
pre
rac
bea

6.2

The
Ne

.: Configuration

nfirm the entr

Rack

then

‘I

nsfer arm (6.

ad at ‘

tower 1’

2.4 Lift

pos

o to the

Manu

wer 1’

and u

sition’

to defin

ck on

Shift positio
(approx. 30

Work positio
(approx. 158

2.5 Needle

special positio

epared method
ck 6.2041.840

aker filled with

2.6 Method

e following m

t:

TitrIC pro I:

T

Depending o
carried out:

Value 1 = 1
ion chromat
Value 1 = 2
a calibration
Value 1 = 3

This method
method in ti

TitrIC pro I_c

for calibratio
used in com

I_ conductiv

of the Swing H

ries with

nitialize Rack

1462.040) is

.

sitions

al’

operation

use the entr

ne suitable va

gure>

each tim

n

for

mm)

on for

8 mm)

e rinse positio

on of the rac

ds, the used

0 this refers t

h ultrapure wa

ds

ethods (.imet

This method is

on the value o

complete an

ography.

only an ion c

n)

only a titratio

d is used in co

iamo

TM

.

conductivity ca

on of the cond

mbination with

ity calibration

.

Head at tower 1

>

and open th

k’

. Wait a few

now mounted

click on

815 S

ries

Rack po

lues for the fo

e):

changing the

aspirating of t

on

ck is used fo

position is nu

to the last po

ter is placed t

files) are pro

s the standard

of

Value 1

the f

nalysis includin

chromatograp

on analysis

ombination wit

alibration:

This

uctivity senso
the tiamo

TM

m

he properties,

w seconds. T

d onto the Sw

Sample Chang

osition’

and

ollowing positi

rack position

the sample

or rinsing. In

mber 59. On

osition. A sam

here.

ovided for Ma

d method.

following will b

ng titration and

hy analysis (e

h the

TitrIC pr

s method is us

or. It has to be

method

TitrIC P

A
In

, go

The

wing

ger /

Lift

ons

the
the

mple

gIC

be

d

e.g.

ro I

sed

Pro

Im

Me

rela
the
No
Alt
pe
fam

6.3

6.4

Co
tia
ge
con
aut
on

6.5

Th
sur
con
10
MS
mo
MS
me
be

Fig

No
Do

Application Bulle

nstallation Instru

TitrIC pro I_t

used to dete
used in tiam
tiamo

TM

me

TitrIC pro I_t

used to dete
solution use
with the tiam

of EDTA

.

port: Click on

ethod manage

ated to TitrIC

e methods in t

ote!

erations of the

rson at the ad

miliar with Mag

Shut down Ma

3 Configurati

tiamo

TM

2.3 is

4 Devices

onnected USB

mo

TM

is start

nerated requ

nfiguration. Ke

tomatically req

.

5 Solution

e solution to

re the Dosino
nnected to the

mL Dosing U

SB 2 of the 90
ol/L TRIS / 0.
SB 3 of the 90
ethods provide

low.

At the left cl
under ‘

Titran

appropriate
under ‘

Solut

.: Configuration

ow the tubing
osing unit unde

tin 353

uctions of TitrIC

titer determinat

ermine the tite

mo. It has to be

ethod

TitrIC pro

titer determinat

ermine the tite

ed in tiamo. It h

mo

TM

method

n

Method

at th

r… / Edit / I

pro I from the

he folder exam

ese methods s

ministrator lev

gIC Net.

agIC Net

ion of tiamo

TM

s started.

devices are a

ted. After con

uest the de

eep the propo

quested to sav

be used must

of the 20 mL

e MSB 1 port

Unit (0.05 mo

5. The Dosino

1 mol/L acety

05. In order to

ed, the solution

ick on ‘

Config

nts/Solutions’

d

(empty) entrie

tion name’

and

table for titrant

g lengths and

er ‘

Edit/Propert

pro I

ation of HCl:

Th

er of the 0.1 m

e used in com

o I_titer determ

ation of EDTA:

er of the 0.05 m

has to be use

TitrIC pro I_tit

he left, then s

Import

Imp

e MagIC Net

mple/TitrIC of

should only be
vel and who is

TM

automatically

nfirmation of t

evices are

osed device na

ve solutions –

t be defined i

Dosing Unit (
of the 905. T

ol/L Na

2

EDTA)

o of the 20 mL
ylacetone) is

o ensure com

n must be nam

uration’

, then

double-click o

es and enter t

d ‘

Concentratio

ts/solutions

d ports are d

rties…/ Dosing

Page 8 o

his method is

mol/L HCl solut

bination with t

mination of HCl

This method i

mol/L Na

2

EDT

d in combinat

er determinatio

select under

F

ort the meth

CD. You will
the CD.

e carried out b

s thoroughly

recognized w

the automatic

stored in

ames. The use

– accept and c

n tiamo

TM

. M

(0.1 mol/L HC

The Dosino of

) is connected

L Dosing Unit

connected to

mpatibility with

med as descri

at the top righ

on the

he following

on’

:

defined for e

unit’

as follow

of 14

tion

the

l

.

s

TA

ion

on

File /

hods

find

by a

when

cally

the

er is

click

Make

Cl) is

the

d to

(0.2

the
the

bed

ht

each

ws: