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Metrohm TitrIC pro I User Manual

Page 11

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8

8.1

For
item

Nu

IC

1

1

1

8.2

A
des

8.3

Po
wit
Do
pur

The
Sa

8.4

The
mo
tran
sec
pie
PT
wh

8.5

The
on
The
Pro

Us
blu
dilu
inje
per
Co
(6.2
don
Thi
pum

The
pro

TitrIC pro –

Delivery pa

r the Dilution

ms:

umber

A

Dilution

2

2

6

2 Installation

short straight

scribed here.

3 Dosino

rt 4 of the Dos
h the FEP As

sing Unit 10

re water bottle

e Dosino is co

mple Process

4 Transfer Tu

e 10 mL Tra

ounted on the

nsfer tubing to

cond end of

ece at the swi

TFE capillary a

ich is used by

5 External Di

e External Dil

the right side

e stirrer is co

ocessor on MS

e the 0.75 m

ue/blue PVC

ution vessel
ection valve o

ristaltic Pump

nnect the det

2744.040) to

ne with the d

is gives the p

mp channels f

e external dil

ocessor, whic

– Combo Kit D

ackage

n setup with T

Article no.

2.800.0010

2.801.0010

6.5338.000

n

t forward des

sino with the 1

spiration tube

mL) and mou

e (6.1608.070)

onnected to M

sor.

ubing

ansfer Tubing

e tower (towe

o port 1 of the

the transfer t

ing arm. If co

and the M6 U

y TitrIC pro I st

lution Vessel

ution vessel w

of the 815 Ro

onnected to t
SB 2.

mm ID PTFE c

pump tubing
via Peristaltic

f the anions IC

p the rinse c

tector outlet w

the MSM rins

detector waste

possibility to u

for pumping th

lution vessel

h is easiest

Dilution

TitrIC you ne

Articl

Dosin

Magn

TitrIC

scription of th

10 mL Dosing

e (6.1829.010

unted directly

).

MSB 1 at the 8

g with holder

r 1). Connect

e 10 mL UPW

tubing is conn

onnected, rem

NF 10/32 cou

tandard setup

l

with all access

obotic USB Sa

he 815 Robo

capillary (6.18

(6.1826.020)

c Pump of t

C. To be able

channel has

with a 2x UNF

se channel. Th

e instead of

use one of the

he sample to t

is mounted o

when the rac

eed the follow

e designation

no

netic Stirrer

C pro equipment

he dilution ki

Unit is equipp

, included in

on the 2 L u

815 Robotic U

(6.1562.130

t one end of

Dosing Unit. T

nected to the

move the 0.75m

upling connec

.

sories is moun

ample Process

otic USB Sam

803.080) and

) to connect

he MSM to

e to use the M

to be remov

F 10/32 coup
he rinsing is n

ultra pure wa

e MSM perista

he loops.

onto the sam

ck is tempora

A
In

wing

t for Dilution

t is

ped

the

ultra

USB

) is

the

The

e T-

mm

ction

nted

sor.

mple

the
the
the

MSM

ved.

pling

now

ater.

altic

mple

arily

rem
the
con
the
125

Fig

8.6

Th
Ne

Application Bulle

nstallation Instru

moved. The e

e needle into t

ntrol (in the w

e swing head a

5 mm.

.: Settings for th

6 Analysis

e following (.i

et:

TitrIC pro I_d

method. De
following wi
Value 1 = 1
ion chromat
Value 1 = 2
a calibration
Value 1 = 3

This method
method in ti

TitrIC pro I_d

is used for c
to be used i

TitrIC pro I_c

TitrIC pro I_d

method is u
HCl solution
combination

determinatio

TitrIC pro I_d

method is u
Na

2

EDTA so

combination

determinatio

tin 353

uctions of TitrIC

exact position

the external d

window manua

angle is ~117

he 815 Robotic

met files) me

dilution:

This m

pending on th

ll be carried ou

complete an

tography.

only an ion c

n)

only a titratio

d is used in co

iamo

TM

.

dilution conduc

calibration of t

n combination

calibration con

diution titer det

sed to determ

n used in tiamo
n with the tiam

on of HCl

.

diution titer det

sed to determ

olution used in

n with the tiam

on of EDTA

.

pro I

can be adju

dilution vessel

al). The appro

7.2°, The work

USB Sample P

ethods are pro

method is the

he value of

Val

ut:

nalysis includin

chromatograp

on analysis

ombination wit

ctivity calibrat

the conductivit
n with the tiam

nductivity

.

etermination of

mine the titer of

o. It has to be

mo

TM

method

T

etermination of

mine the titer of

n tiamo. It has

mo

TM

method

T

Page 11 o

sted by direc

l with the man

oximate value

k position is ab

rocessor XL

ovided for Ma

standard

lue 1

the

ng titration and

phy analysis (e

th

TitrIC pro I

ion:

This meth

ty sensor. It ha

mo

TM

method

f HCl:

This

f the 0.1 mol/L

used in

TitrIC pro I_tite

f EDTA:

This

f the 0.05 mol

s to be used in

TitrIC pro I_tite

of 14

cting

nual

e for

bout

agIC

d

e.g.

hod

as

L

er

/L

n

er