Metrohm TitrIC pro I User Manual
Page 12
Application Bulletin 353
Installation Instructions of TitrIC pro I
Page 12 of 14
The following methods (.mmet files) are provided for
tiamo
TM
:
TitrIC pro I:
This method is the standard method used. It
does the complete titration analysis and sends the
results to MagIC Net. It is used in combination with
TitrIC pro I_dilution
method in MagIC Net.
In tiamo
TM
it is typically used as a single determination
in autorepeat mode. In other words, it is always ready
to do a titration as soon MagIC requires it. To set it into
autorepeat go to the Run window, right-mouse-click and
select
Properties Run window
. Under Process select
Autorepeat determination
. Close the window with
.
TitrIC pro I_pH calibration manual:
Here the iAquatrode
is taken out of the titration vessel and placed into the
buffer solutions. Start this method only from tiamo
TM
!
TitrIC pro I_titer determination of HCl:
This method is
used for the titer determination. It has to be used in
combination with the MagIC Net method
TitrIC pro
I_dilution titer determination of HCl
.
TitrIC pro I_titer determination of EDTA:
This method is
used for the titer determination. It has to be used in
combination with the MagIC Net method
TitrIC pro
I_dilution titer determination of EDTA
.
TitrIC pro I_conductivity calibration:
This method is used
for calibration of the conductivity sensor. It has to be
used in combination with the MagIC Net method
TitrIC
pro I_dilution calibration conductivity
.
With the TitrIC pro – Combo Kit Dilution following analysis
can be carried out using the TitrIC pro I_dilution methods in
MagIC respectively tiamo
TM
:
The whole procedure is controlled by the MagIC Net
software which is the master software. In tiamoTM the
method TitrIC pro I is selected as a single determination.
Start the determination in autorepeat mode. To set it into
autorepeat go to the Run window, right-mouse-click and
select
Properties Run window
. Under Process select
Autorepeat determination
. Close the window with
. Start
the determination. Now tiamo
TM
is waiting for the start
signal from MagIC Net via RS232.
In the MagIC Net software select the method
TitrIC pro
I_dilution
. Enter the required sample position, sample
identification etc. into MagIC Net. For value 1 choose
according to the list below:
Value 1 = 1 complete analysis including titration and
ion chromatography.
Value 1 = 2 only an ion chromatography analysis (e.g.
a calibration)
Value 1 = 3 only a titration analysis
With Value 1 = 1 a complete analysis is carried out.
Depending on the entered dilution factor the following will be
done:
Dilution Factor = 1:
Depending on the measured conductivity an appropriate
dilution factor is automatically applied by MagIC Net. The
calculation factor is calculated according to Time Program
No. 2. The finally used dilution factor is the integer of the
conductivity divided by 250.
Dilution Factor >1:
If a dilution factor is known it can be directly entered into the
sample table. It will be diluted accordingly. The conductivity
measurement has no influence on the dilution in this case.
E.g. with Value 1 = 2 an ion chromatographic analysis will
be carried out with the entered dilution factor. No dilution
factor will be calculated