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Metrohm 940 Professional IC Vario ONE/SeS/PP/HPG User Manual

Page 6

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Table of contents

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IV

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940 Professional IC Vario ONE/SeS/PP/HPG (2.940.1540)

3.13.2

Connecting the suppressor .................................................... 34

3.14 Peristaltic pump .................................................................. 38
3.14.1

Installing the peristaltic pump ................................................ 38

3.14.2

Mode of operation for the peristaltic pump ........................... 44

3.15 Metrohm CO

2

Suppressor (MCS) ....................................... 45

3.15.1

General information on MCS ................................................. 45

3.15.2

Connecting the MCS ............................................................. 46

3.15.3

Installing adsorption cartridges .............................................. 47

3.16 Installing the detector ........................................................ 49

3.17 Connecting the sample degasser (optional) ..................... 49

3.18 Installing the high-pressure gradient module .................. 51

3.19 Connecting the instrument to a computer ....................... 51

3.20 Connecting the instrument to the power supply ............. 52

3.21 Initial start-up ..................................................................... 53

3.22 Connecting and rinsing the guard column ....................... 56

3.23 Connecting the separation column ................................... 58

3.24 Conditioning ........................................................................ 61

4 Operation

63

5 Operation and maintenance

64

5.1

IC system ............................................................................. 64

5.1.1

Operation .............................................................................. 64

5.1.2

Care ...................................................................................... 64

5.1.3

Maintenance by Metrohm Service .......................................... 64

5.1.4

Shutting down and starting back up ...................................... 65

5.2

Capillary connections ......................................................... 66

5.3

Servicing the door .............................................................. 66

5.4

Column thermostat – Replacing the capillaries ............... 66

5.5

Handling the eluent ............................................................ 68

5.5.1

Manufacturing eluent ............................................................ 68

5.5.2

Changing the eluent .............................................................. 69

5.6

Servicing the eluent degasser ........................................... 69

5.7

Notes on operating the high-pressure pump ................... 70

5.8

Servicing the high-pressure pump .................................... 71

5.9

Servicing the inline filter .................................................... 84

5.10 Servicing the pulsation absorber ...................................... 87

5.11 Injection valve ..................................................................... 87

5.12 Suppressor .......................................................................... 87
5.12.1

Notes for operating the suppressor ........................................ 87