Thermo Fisher Scientific Ion Selective Electrodes Calcium User Manual
Page 16

Calcium Electrode
Instruction Manual
16
5.
If another electrode is not available for test purposes, or if the electrode in use is suspect,
review the instruction manual and be sure to:
- Clean and rinse the electrodes thoroughly.
- Prepare the electrodes properly.
- Use the proper filling solution.
- Adjust the pH of the solution according to the method being used for the analysis.
- Measure correctly and accurately.
- Review
TROUBLESHOOTING HINTS.
Standards and Reagents
Whenever problems arise with the measuring procedure that has been used successfully in the past,
be sure to check the standard and reagent solutions. If in doubt about the credibility of any of the
solutions, prepare them again. Errors may result from contamination of the ISA, incorrect dilution
of standards, poor quality distilled/deionized water, or a simple mathematical miscalculation.
Sample
Look for possible interferences, complexing agents, or substances which could affect the response
or physically damage the sensing electrode (or the reference electrode) if the electrodes work
perfectly in the standard, but not in the sample.
Try to determine the composition of the samples prior to testing to eliminate a problem before it
starts. (See
Measuring Hints, Sample Requirements,
and
Interferences
.)
Technique
Be sure that the electrodes' limit of detection has not been exceeded. Be sure that the analysis
method is clearly understood and is compatible with the sample. Refer to the instruction manual
again. Reread
GENERAL PREPARATION
and
ELECTRODE CHARACTERISTICS
.
If trouble still persists, call Eutech Instruments Pte Ltd. at (65) 6778-6876 and ask for the Customer
Services Department.