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Startup using vacuum, A) to fill the system, Procedure: actions – Bronkhorst CEM W-300B User Manual

Page 19

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Startup using Vacuum

A) To fill the system:

Procedure:

Actions:

A1) Evacuate the lines “Vacuum”

Start pumps

A2) Evacuate all lines

Close: 2,3,5,10 and 9.

Connect inert gas on carrier gas inlet.

Open : 1,4,7,11.

Give setpoint to gas and liquid control

(the control valves 6 and 8 open).

Pump for a long time.

Remark: if the system is not completely

dry follow procedure of E3, E4, (E5).

A3) Purge line between inert gas source and

valve 2.

Close: 4.

Open valve 2 briefly for some seconds.

A4) Purge line between process gas source and

gas MFC.

Give setpoint = 0 to LFM (6 closes).

Open valve 9 briefly for some seconds.

A5) Pump down liquid supply.

Open 3 for some time, close 3.

A6) Pressurize liquid supply.

Close 1, give right pressure on inert gas

supply. Open 2, open 3 briefly.

A7) Fill the system with liquid.

(1)

Let gas flow in the carrier gas line during

filling of the system.

Close 7.

Open 5 briefly, allow mixing valve 6 to fill.

A8) Optional: degassing mixing valve.

Open 7, a needle valve will be best, to

avoid too much liquid be pumped away.

A9) The system is now ready for use.

Vacuum

Liquid

1

4

3

5

6

8

10

11

9

MFC

Carrier

Processgas

Vacuum

7

LFM

Inertgassupply

2

Process

Vacuum

Valve

Heatedline

CEM

Liquid

Gas

App. 1, page 3

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