beautypg.com

Metrohm 940 Professional IC Vario ONE/SeS/PP/Prep 1 User Manual

Page 6

background image

Table of contents

■■■■■■■■■■■■■■■■■■■■■■

IV

■■■■■■■■

940 Professional IC Vario ONE/SeS/PP/Prep 1 (2.940.1510)

3.13.2

Connecting the suppressor .................................................... 33

3.14 Peristaltic pump .................................................................. 37
3.14.1

Installing the peristaltic pump ................................................ 37

3.14.2

Mode of operation for the peristaltic pump ........................... 43

3.15 Metrohm CO

2

Suppressor (MCS) ....................................... 44

3.15.1

General information on MCS ................................................. 44

3.15.2

Connecting the MCS ............................................................. 45

3.15.3

Installing adsorption cartridges .............................................. 46

3.16 Installing the detector ........................................................ 48

3.17 Connecting the sample degasser (optional) ..................... 48

3.18 Connecting the instrument to a computer ....................... 50

3.19 Connecting the instrument to the power supply ............. 51

3.20 Initial start-up ..................................................................... 52

3.21 Connecting and rinsing the guard column ....................... 54

3.22 Connecting the separation column ................................... 56

3.23 Conditioning ........................................................................ 60

4 Operation

62

5 Operation and maintenance

63

5.1

IC system ............................................................................. 63

5.1.1

Operation .............................................................................. 63

5.1.2

Care ...................................................................................... 63

5.1.3

Maintenance by Metrohm Service .......................................... 63

5.1.4

Shutting down and starting back up ...................................... 64

5.2

Capillary connections ......................................................... 65

5.3

Servicing the door .............................................................. 65

5.4

Column thermostat – Replacing the capillaries ............... 65

5.5

Handling the eluent ............................................................ 67

5.5.1

Manufacturing eluent ............................................................ 67

5.5.2

Changing the eluent .............................................................. 68

5.6

Servicing the eluent degasser ........................................... 68

5.7

Notes on operating the high-pressure pump ................... 69

5.8

Servicing the high-pressure pump .................................... 70

5.9

Servicing the inline filter .................................................... 83

5.10 Servicing the pulsation absorber ...................................... 86

5.11 Injection valve ..................................................................... 86

5.12 Suppressor .......................................................................... 86
5.12.1

Notes for operating the suppressor ........................................ 86

5.12.2

Taking care of the suppressor housing ................................... 87