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Metrohm 930 Compact IC Flex ChS User Manual

Page 6

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Table of contents

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IV

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930 Compact IC Flex ChS (2.930.1200)

3.13 Connecting the instrument to the power supply ............. 37

3.14 Initial start-up ..................................................................... 38

3.15 Connecting and rinsing the guard column ....................... 40

3.16 Connecting the separation column ................................... 42

3.17 Conditioning ........................................................................ 45

4 Operation

47

5 Operation and maintenance

48

5.1

IC system ............................................................................. 48

5.1.1

Operation .............................................................................. 48

5.1.2

Care ...................................................................................... 48

5.1.3

Maintenance by Metrohm Service .......................................... 48

5.1.4

Shutting down and starting back up ...................................... 49

5.2

Capillary connections ......................................................... 50

5.3

Servicing the door .............................................................. 50

5.4

Handling the eluent ............................................................ 50

5.4.1

Manufacturing eluent ............................................................ 51

5.4.2

Changing the eluent .............................................................. 51

5.5

Notes on operating the high-pressure pump ................... 52

5.6

Servicing the high-pressure pump .................................... 53

5.7

Servicing the inline filter .................................................... 66

5.8

Servicing the pulsation absorber ...................................... 69

5.9

Injection valve ..................................................................... 69

5.10 Suppressor .......................................................................... 69
5.10.1

Notes for operating the suppressor ........................................ 69

5.10.2

Taking care of the suppressor housing ................................... 70

5.10.3

Servicing the suppressor ........................................................ 70

5.11 Servicing the detector ........................................................ 77

5.12 Rinsing the sample path .................................................... 77

5.13 Separation column ............................................................. 78
5.13.1

Separating efficiency .............................................................. 78

5.13.2

Protecting the separation column .......................................... 79

5.13.3

Storing the separation column ............................................... 79

5.13.4

Regenerating the separation column ...................................... 79

5.14 Quality Management and qualification with

Metrohm ............................................................................. 80

6 Troubleshooting

81

6.1

............................................................................................. 81