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Parr Instrument Series 4580 User Manual

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TABLE OF CONTENTS

Related

Instructions .........................2

Customer

Service ............................2

Preface..................................................3
Scope...............................................3
Safety

Information............................3

General

Specifications.....................3

Explanation of Symbols ...................4

Environmental

Conditions................4

Provisions for Lifting and

Carrying ...........................................4

Cleaning & Maintenance..................4

Intended

Usage ...............................5

User’s

Responsibility .......................5

Unpack

Carefully .............................5

Fixed Head or Removable
Head Design.........................................6

Flat Flexible Graphite Gasket ..........6

Installation............................................7

Pressure and Temperature

Limits................................................7

Assemble the Reactor.........................8

Heaters .................................................10

Identify the Valves ...............................11

Gas Inlet Valves...............................11
Gas Release Valve ..........................11
Liquid Sampling Valve .....................11

Other Vessel Head Fittings.................12
Safety

Rupture Disc.........................12

Type J Thermocouple ......................12

Pressure

Gage.................................12

Gage and Valve Adapters................12

How to Use the Vessel ........................13

Fixed Head Vessels.........................13

Removable Head Vessels ...............13

Gas

Connections .............................14

Pressurizing the Vessel ...................14

Do Not Overfill the Vessel................14

Releasing

Pressure .........................15

Withdrawing Liquid Samples ...........15

Initial

Operating Test........................15



Accessories .........................................16
Pneumatic Lift ..................................16
Internal

Cooling Loop.......................17

Liners ...............................................17

Spare Parts Kit.................................17

Air

Motor ..........................................17

Variable Speed Electric Motor .........18

Explosion Proof Operation.................19

Periodic Pressure Tests .....................20

General Maintenance Notes ...............21

Parts Lists ............................................22

Reaction Vessel Parts List...............22

4580 Head Assembly Front View ....24

4580 Head Assembly Rotated View 25

Overarm Parts List...........................26

Related Instructions

The following Parr publications are also

available to further your understanding of this
instrument and its component parts:

No.

Description

230M Safety Precautions to be observed

when operating Pressure Reaction
Equipment

231M Operating Instructions for Parr Safety

Rupture Discs

285M Sealing Instructions for Flexible

Graphite Gaskets

548M Operating Instructions for Series 4848

Reactor Controllers

234M Operating and Maintenance

Instructions for Parr Magnetic Drives

323M Operating Instructions for Parr

Pressure Relief Valves

201M Limited Warranty
F0042 Health & Safety Assurance Certification

Customer Service

Questions concerning the installation

or operation of this instrument can be
answered by the Parr Customer Service
Department:
Phone:

309-762-7716

800-872-7720
Fax:

309-762-9453

www.parrinst.com

[email protected]