Hanna Instruments HI 96732 - Manual

1. GLP/ key: press to enter GLP mode. In calibration mode press to
edit the date and time.
2. CAL CHECK key: press to perform the validation of the meter, or
press and hold for three seconds to enter calibration mode.
3. ZERO/CFM key: press to zero the meter prior to measurement, to
confirm edited values or to confirm factory calibration restore.
4. READ/ key: In measurement mode, press to make a measurement.
In GLP mode press to view the next screen.
5. ON/OFF key: to turn the meter on and off.
6. Liquid Crystal Display (LCD)
7. Cuvette alignment indicator
8. Cuvette holder
DISPLAY ELEMENTS DESCRIPTION:
INSTRUCTION MANUAL
HI 96732 HI 96732 HI 96732 HI 96732 HI 96732
w w w . h a n n a i n s t . c o m
Preliminary examination:
Please examine this product carefully. Make sure that the instrument is
not damaged. If any damage occured during shipment, please notify
your Dealer.
Each HI 96732 Ion Selective Meter is supplied complete with:
• Two Sample Cuvettes and Caps
• 9V Battery
• Instruction Manual
Note:
Save all packing material until you are sure that the instrument
works correctly. Any defective item must be returned in its original
packing.
For more details about spare parts and accessories
see “Accessories”.
Dear Customer,
Thank you for choosing a Hanna product. This manual will provide you
with the necessary information for the correct use of the instrument. Please
read it carefully before using the meter. If you need additional technical
information, do not hesitate to e-mail us at [email protected]. Functional description:
Light High: There is too much light to perform
a measurement. Please check the preparation of
the zero cuvette.
Light Low: There is not enough light to perform
a measurement. Please check the preparation of
the zero cuvette.
No Light: The instrument cannot adjust the
light level. Please check that the sample does
not contain any debris.
Inverted cuvettes: The sample and the zero
cuvette are inverted.
Zero: A zero reading was not taken. Follow the
instructions of the measurement procedure for
zeroing the meter.
Under range: A blinking “0.00” indicates that
the sample absorbs less light than the zero
reference. Check the procedure and make sure
you use the same cuvette for reference (zero)
and measurement.
Over Range: A flashing value of the maximum
concentration indicates an over range condition.
The concentration of the sample is beyond the
programmed range: dilute the sample and
re-run the test.
Standard Low: The standard reading is less
than expected.
Standard High: The standard reading is higher
than expected.
Errors and warnings:
Measurement procedure:
1• Turn the meter on by pressing ON/OFF.
2• When the beeper sounds briefly and the
LCD displays dashes, the meter is ready.
The blinking “ZERO” indicates that the
instrument needs to be zeroed first.
3• Fill one 60 mL glass bottle completely with
the unreacted sample. Replace the cap and
ensure that a small part of the sample spills
over.
4• Remove the cap and add 5 drops of HI
93732A-0 and 5 drops of HI 93732B-0.
Add some more sample, to fill the bottle
completely. Replace the cap again and
ensure that a part of the sample spills over.
This is to make sure that no air bubbles
have been trapped inside, wich would corrupt
the reading.
5• Invert several times the bottle. The sample
becomes orange-yellow and a flocculant agent
will appear. Let the sample stand and the
flocculant agent will start to settle.
6• After approximately 2 minutes, when the
upper half of the bottle becomes limpid,
add 10 drops of HI 93732C-0.
7• Replace the cap and invert the bottle until
dissolution of the settled flocculant is complete.
The sample is ready for measurement when
it is yellow and completely limpid.
8• Fill the cuvette up to the mark with 10 mL
of the unreacted (original) sample, and
replace the cap. This is the blank.
9• Place the cuvette into the holder and ensure
that the notch on the cap is positioned
securely into the groove.
10•Press ZERO/CFM and the lamp, cuvette and
detector icons will appear on the display,
depending on the measurement phase. After
a few seconds the display will show “-0.0-”.
The meter is now zeroed and ready for
measurement. Remove the cuvette.
Measurement
1. The measuring scheme (lamp, cuvette, detector), appears during
different phases of zero or reading measurement
2. Error messages and warnings
3. The battery icon indicates the charge state of the battery
4. The hourglass appears when an internal check is in progress
5. Status messages
6. The chronometer appears when the reaction timer is running
7. The month, day and date icons appear when a date is displayed
8. Four digit main display
9. Measuring units
10. Four digit secondary display
ON ZERO READING:
ON SAMPLE READING:
DURING CALIBRATION PROCEDURE:
OTHER ERRORS AND WARNINGS:
Cooling lamp: The instrument waits for the
lamp to cool down.
Battery low: The battery must be replaced soon.
Dead battery: This indicates that the battery
is dead and must be replaced. Once this
indication is displayed, normal operation of the
instrument will be interrupted. Change the
battery and restart the meter.
Cap error: Appears when external light enters
in the analysis cell. Assure that the cuvette cap
is present.
Dissolved Oxygen
ISM
2
9
Technical specifications:
Range 0.0 to 10.0 mg/L
Resolution 0.1 mg/L
Accuracy ±0.4 mg/L ±3% of reading @ 25°C
Typical EMC Dev. ±0.1 mg/L
Light Source Light Emitting Diode
Light Detector Silicon Photocell with 466 nm filter
Method Adaptation of the Standard Methods for
Examination of Water and Wastewater (18
th
edition), azide modified Winkler method.
The reaction between dissolved oxygen
and the reagent causes a yellow tint in the
sample.
Environment 0 to 50°C (32 to 122°F);
max 95% RH non-condensing
Battery Type 1 x 9 volt
Auto-Shut off After 10' of non-use in measurement mode;
after 1 hour of non-use in calibration mode;
with last reading reminder.
Dimensions 192 x 104 x 69 mm (7.6 x 4.1 x 2.7”)
Weight 360 g (12.7 oz.).
3
4
5
6
10 mL
sample
7
8
10