Metrohm 930 Compact IC Flex Oven/SeS - Manual (Page 6)

Table of contents
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IV ￭￭￭￭￭￭￭￭
930 Compact IC Flex Oven/SeS (2.930.2400)
3.12.2 Connecting the MCS ............................................................. 37
3.12.3 Installing adsorption cartridges .............................................. 38
3.13 Installing the detector ........................................................ 40
3.14 Connecting the instrument to a computer ....................... 40
3.15 Connecting the instrument to the power supply ............. 41
3.16 Initial start-up ..................................................................... 42
3.17 Connecting and rinsing the guard column ....................... 45
3.18 Connecting the separation column ................................... 47
3.19 Conditioning ........................................................................ 50
4 Operation 52
5 Operation and maintenance 53
5.1 IC system ............................................................................. 53
5.1.1 Operation .............................................................................. 53
5.1.2 Care ...................................................................................... 53
5.1.3 Maintenance by Metrohm Service .......................................... 53
5.1.4 Shutting down and starting back up ...................................... 54
5.2 Capillary connections ......................................................... 55
5.3 Servicing the door .............................................................. 55
5.4 Column oven – replacing the capillaries ........................... 55
5.5 Handling the eluent ............................................................ 57
5.5.1 Manufacturing eluent ............................................................ 57
5.5.2 Changing the eluent .............................................................. 58
5.6 Notes on operating the high-pressure pump ................... 58
5.7 Servicing the high-pressure pump .................................... 59
5.8 Servicing the inline filter .................................................... 72
5.9 Servicing the pulsation absorber ...................................... 75
5.10 Injection valve ..................................................................... 75
5.11 Suppressor .......................................................................... 75
5.11.1
Notes for operating the suppressor ........................................ 75
5.11.2 Taking care of the suppressor housing ................................... 76
5.11.3 Servicing the suppressor ........................................................ 76
5.12 Servicing the Metrohm CO
2
Suppressor (MCS) ................ 83
5.12.1 Replacing the CO
2
adsorption cartridge ................................. 83
5.12.2 Regenerating the H
2
O adsorption cartridge ............................ 83
5.13 Servicing the detector ........................................................ 84
5.14 Rinsing the sample path .................................................... 84
5.15 Separation column ............................................................. 85
5.15.1
Separating efficiency .............................................................. 85