Parr Instrument Series 4530 - Manual (Page 2)

Floor Stand Reactors
P a r r I n s t r u m e n t C o m p a n y 2
Table of Contents
PREFACE
Scope — 3
Related Instructions — 3
Safety Information — 3
General Specifi cations — 3
Electrical Ratings— 3
Explanation of Symbols — 4
Environmental Conditions — 4
Provisions for Lifting and Carrying — 4
Intended Usage — 4
Cleaning & Maintenance — 4
User’s Responsibility — 5
Unpack Carefully — 5
INSTALLATION
Pressure and Temperature Limits — 6
ASSEMBLE THE REACTOR — 6
IDENTIFY THE VALVES
Gas Inlet Valve — 8
Gas Release Valve — 8
Liquid Sampling Valve — 8
OTHER VESSEL HEAD FITTINGS
Safety Rupture Disc — 9
Type J Thermocouple — 9
Gage and Valve Adapters — 9
HOW TO USE THE VESSEL
Fixed Head Vessels — 10
To open the Vessel — 10
Before Closing the Vessel— 10
To Close the Vessel— 10
Removable Head Vessels — 10
To Open the Vessel— 10
Before Closing the Vessel— 10
To Close the Vessel— 10
Sealing Vessels with PTFE Gaskets— 10
Gas Connections— 10
Pressurizing the Vessel — 11
Do Not Overfi ll the Vessel— 11
Releasing Pressure— 11
Withdrawing Liquid Samples— 11
Initial Operating Test— 11
ACCESSORIES
Internal Cooling Coils — 12
Variable Speed Electric Motor — 12
Air Motor — 12
Liners — 12
Spare Parts Kit — 12
EXPLOSION PROOF OPERATION — 13
PERIODIC PRESSURE TESTS — 13
GENERAL MAINTENANCE NOTES — 14
PARTS LISTS
Internal Fittings — 16
External Fittings — 17
Removable Head Style Parts Lists — 18
Fixed Head Style Parts Lists — 20
OVERARM PARTS LIST — 23
COOLING COIL PARTS LIST — 25
HEATERS PARTS LIST — 26
Customer Service
Questions concerning the installation or operation of this instrument
can be answered by the Parr Customer Service Department:
1-309-762-7716 • 1-800-872-7720 • Fax: 1-309-762-9453
E-mail: [email protected] • http://www.parrinst.com