3 setting up application parameters, 4 how to perform a wet application, Warning – BUCHI Wet Digester B-440 User Manual
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6 Operation
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B-440 Operation Manual, Version D
6.3
Setting up application parameters
Internal program storage
The B-440 is capable of storing 9 application methods in its program storage.
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Each program has 5 steps with individual parameter pairs of time and temperature.
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Parameter name
Range
Programs
1 – 9
Steps
1 – 5
Temperature
ambient – 600 °C
Time (per "STEP")
0 – 240 minutes
Setting up PROGRAMs and STEPs
Switch "ON" the Wet Digester.
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๗After the bootprocess ( 4 seconds) the instrument will be operational.
Select a program via the right "SELECT" button (below "PROGRAM" display).
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Press the left "SELECT" button (below "STEP" display) repeatingly to switch through every
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"TIME" / "TEMP" parameter of each "STEP" in a loop.
๗The "STEP" display shows the selected step (1—5 ).
๗The corresponding "TIME" / "TEMP" display will flash for 10 seconds and switch to "STEP" level 1
without button action.
To change either the heating time or temperature of a step, use the "UP" and "DOWN" buttons
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while the respective display flashes.
๗As soon as the display stops flashing, the value is being stored.
NOTE
Some application methods do not require a full set of 5 steps. To disable a "STEP", set its "TIME "
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to 0.
During a running application, programming is not possible.
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6.4
How to perform a wet application
Digestion fumes can be hazardous and must be neutralized by a Scrubber or a condensate
trap / Scrubber combination. Fumes which may escape during operation must be safely withdrawn by
a fume hood! Wear personal protective equipment, see section 2.5 for general safety information!
!
WARNING
Death or serious poisoning by contact or incorporation of harmful substances and fumes at use.
Before operation, check the instrument for correct assembling
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Rinse condensate trap, hoses and connectors before use
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Before operation inspect sealing surfaces and tubes for good condition and tightness
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Secure all hoses with hose clamps
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Exchange worn out or defective parts immediately
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Only operate the instrument in a fume hood
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Directly withdraw released gases and gaseous substances by a Scrubber
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Dispose of condensate in tubings and glassware safely after use
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Do not inhale digestion fumes
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